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Breck continued his investigation following his doctoral studies and, in 1968, he demonstrated a method for synthesizing molecular sieve zeolites in water. He demonstrated that the synthesis of molecular sieves could be performed in the laboratory under a variety of competitive conditions while preserving purity. The objective was to develop a molecular sieve synthesis that did not require isolation and pretreatment of syrups as in the patent process. This demonstration was a significant improvement on the patent process, which also depended on a basic chelating agent. This was a first step toward a process that could be readily scaled up.
This study, reported as IMA-1917, represents a landmark in the synthesis of zeolites because it is the first to describe a recipe for synthesizing molecular sieves from methanol. The recipe for synthesizing zeolite was completely new and unexpectedly successful. Further developments resulted in the introduction of commercial zeolite production that, from the beginning, was a source of energy savings for the conversion of methanol to gasoline. After a period of waiting for the invention, a number of patents were granted in various countries for different processes of preparing molecular sieves. Examples of such patents are US letter patent No. 3,140,249 of First et al., US patent 3,140,251 of Burress et al., US patent 3,140,253 of Turnbull, US patent 3,140,699 of Mountain, US patent 3,140,701 of Schatschneider et al., US patent 3,140,752 of Hayes et al., US patent 3,140,754 of O’Neal et al., US patent 3,140,755 of Givens et al., US patent 3,140,759 of Linder et al., US patent 3,140,808 of Mountain, and US patent 3,140,834 of Vedeckis et al. These patents covered processes of preparing molecular sieve zeolites in coprocesses with petrochemical feedstocks, such as olefins and benzene. d2c66b5586
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